HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 2-(2',6'-Diisopropylphenylazo)-4,6-ditertbutylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2,4-Di-tert-butylphenol | HCID 7311 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Diisopropylaniline | HCID 32484 | — |
| Reactant | Phenolate | HCID 119047 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-(2',6'-Diisopropylphenylazo)-4,6-ditertbutylphenol | HCID 135723497 | — |
Reaction Steps
This phenol was prepared, as described for above, from a theoretical yield of 7.4 mmol of diazotized 2,6-diisopropylaniline and a phenolate solution comprised of 2,4-Ditertbutylphenol (1.42 g), water (15 mL), NaOH (0.5 g), pyridine (3 mL), and toluene (6 mL) Yield=0.98 g (36%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094848B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-327e3218e975482ebbe892dcbab483af |
| Source note | uspto-grants-2006_08 |