HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3R)-1-benzylpyrrolidin-3-amine → HCID 70032808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3R)-1-benzylpyrrolidin-3-amine | HCID 1519354 | — |
| Reactant | HCID 70033043 | HCID 70033043 | — |
| Product | HCID 70032808 | HCID 70032808 | 30% |
Reaction Steps
The compound of Example 3b was synthesized in a manner similar to the synthesis of the compound of Example 3a, but using (R)-3-amino-1-benzylpyrrolidine as the amine in the last step. Cleavage of 100 mg of functionalized resin (0.52 mmol/g) and purification by RP-HPLC provided 10.5 mg (30%) of the title compound as a white powder. MS (M+H)+=602.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06525044B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-047740b1add946fb863d0532f9321765 |
| Source note | uspto-grants-2003_02 |