HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanemethylamine → HCID 70033211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanemethylamine | HCID 76688 | — |
| Reactant | HCID 70033043 | HCID 70033043 | — |
| Product | HCID 70033211 | HCID 70033211 | 32% |
Reaction Steps
The compound of Example 3f was synthesized in a manner similar to the synthesis of the compound of Example 3a, but using cyclohexylmethylamine as the amine in the last step. Cleavage of 100 mg of functionalized resin (0.53 mmol/g) and purification by RP-HPLC provided 9.0 mg (32%) of the title compound as a white powder. MS (M+H)+=539.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06525044B2 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-ee61fa097d354a0997373f5e9211dfa7 |
| Source note | uspto-grants-2003_02 |