HRID1060689

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CN(C)c1ccc(N=Nc2ccc(S(=O)(=O)Cl)cc2)cc1

HCID91660

Benzenesulfonyl chloride, 4-[2-[4-(dimethylamino)phenyl]diazenyl]-

C14H14ClN3O2S

HCID12972960

未命名化合物

PRODUCTS

生成物

结构：CCOCc1nc2c(N)nc(C)cc2n1CCCCNS(=O)(=O)c1ccc(/N=N/c2ccc(N(C)C)cc2)cc1

HCID178467654

未命名化合物

PROCEDURE

实验过程

Using the method of Examples 32-46, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 1-(4-aminobutyl)-2-ethoxymethyl-6-methyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired product. The observed accurate mass was 565.2720.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-ce6ac4ec9e9e468397ee19eb87d184ec
来源数据集: uspto-grants-2003_02
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06525064B1
来源说明: uspto-grants-2003_02

反应 SMILES

[CH3:1][N:2]([C:4]1[CH:9]=[CH:8][C:7]([N:10]=[N:11][C:12]2[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=2)=[CH:6][CH:5]=1)[CH3:3].[NH2:22][CH2:23][CH2:24][CH2:25][CH2:26][N:27]1[C:35]2[CH:34]=[C:33]([CH3:36])[N:32]=[C:31]([NH2:37])[C:30]=2[N:29]=[C:28]1[CH2:38][O:39][CH2:40][CH3:41]>>[NH2:37][C:31]1[C:30]2[N:29]=[C:28]([CH2:38][O:39][CH2:40][CH3:41])[N:27]([CH2:26][CH2:25][CH2:24][CH2:23][NH:22][S:18]([C:15]3[CH:16]=[CH:17][C:12](/[N:11]=[N:10]/[C:7]4[CH:8]=[CH:9][C:4]([N:2]([CH3:3])[CH3:1])=[CH:5][CH:6]=4)=[CH:13][CH:14]=3)(=[O:20])=[O:19])[C:35]=2[CH:34]=[C:33]([CH3:36])[N:32]=1