HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(6-Chloronaphth-2-ylsulphonyl)piperazine hydrochloride → 1-[4-(1-Tert-butoxycarbonyl-1,2,3,6-tetrahydropyridin-4-yl)benzoyl]-4-[(6-chloronaphthalen-2-yl)sulfonyl]piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(6-Chloronaphth-2-ylsulphonyl)piperazine hydrochloride | HCID 22709766 | — |
| Reactant | 4-(1-tert-Butoxycarbonyl-1,2,3,6-tetrahydropyridin-4-yl)benzoic acid | HCID 22710270 | — |
| Product | 1-[4-(1-Tert-butoxycarbonyl-1,2,3,6-tetrahydropyridin-4-yl)benzoyl]-4-[(6-chloronaphthalen-2-yl)sulfonyl]piperazine | HCID 22711543 | — |
Reaction Steps
In a similar manner to Referential Example 12 except for the use of 4-(1-tert-butoxycarbonyl-1,2,3,6-tetrahydropyridin-4-yl)benzoic acid and 1-[(6-chloronaphthalen-2-yl)sulfonyl]piperazine hydrochloride as the raw materials, the reaction was conducted, whereby the title compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06525042B1 |
| Source dataset | uspto-grants-2003_02 |
| ORD ID | ord-4953b4ea1b024cedbfa3660c35439093 |
| Source note | uspto-grants-2003_02 |