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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 10611Generated: October 25, 2026

1,2-Dodecanediol → 2-Decyl-2,3-dihydrothieno[3,4-b][1,4]dioxine

https://huagongshe.com/reaction/10611

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2-DodecanediolHCID 92866—
Reactant3,4-DimethoxythiopheneHCID 3613501—
Product2-Decyl-2,3-dihydrothieno[3,4-b][1,4]dioxineHCID 9856993—

Reaction Steps

Racemic 2-n-decyl-2,3-dihydro-thieno[3,4-b][1,4]dioxine was synthesized by transetherification of 3,4-dimethoxythiophene with racemic 1,2-dodecanediol as described in EXAMPLE 1. It was characterized by GC-MS and H-NMR-spectroscopy, and exhibited no optical rotation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07094865B2
Source datasetuspto-grants-2006_08
ORD IDord-ea20d853f7c44473a5eaaef5b2e39442
Source noteuspto-grants-2006_08