N-(2-(4-Bromophenyl)propyl)propane-2-sulfonamide → HCID 21893383, compound

HRID 1061155Notes

Reaction equation

HRID 1061155 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([CH:8]([CH3:17])[CH2:9][NH:10][S:11]([CH:14]([CH3:16])[CH3:15])(=[O:13])=[O:12])=[CH:4][CH:3]=1.[CH:18]1([Mg]Cl)[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1>>[CH:18]1([C:2]2[CH:7]=[CH:6][C:5]([CH:8]([CH3:17])[CH2:9][NH:10][S:11]([CH:14]([CH3:16])[CH3:15])(=[O:13])=[O:12])=[CH:4][CH:3]=2)[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19]1

Participants

3

Reactant 2

HCID 9927066N-(2-(4-Bromophenyl)propyl)propane-2-sulfonamideHCID 178478990HCID 178478990, compound

Product 1

HCID 21893383HCID 21893383, compound

Procedure

The title product was prepared from the product of Example 27 as described in Example 15, Condition 2, with the exception that cyclohexylmagnesium chloride was used instead of cyclopentylmagnesium bromide.

Sources & evidence

ORD record
ord-724ec3fd36664afc8132a51d28e220fd
Source dataset
uspto-grants-2003_02
Patent number
US06525099B1

Reaction notes

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