2,4-Dichlorophenethylamine → HCID 22285014, compound

Participants

Reaction Conditions

Reaction Steps

2-(2,4-dichlorophenyl)ethanamine was suspended in toluene with 4-nitrophthalic anhydride (1 eq) and heated to 150° C. After 2 hours, the reaction was cooled and checked for completion by LC/MS. The solvent was then removed in vacuo and the resulting product was taken on to the next step without further purification. Rt 3.36 minutes (HP LCMS), LC/MS m/z 365.1 (MH+).

Provenance & Evidence