HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(neopentyl glycolato)diboron → HCID 22285299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(neopentyl glycolato)diboron | HCID 2734316 | — |
| Reactant | HCID 22285318 | HCID 22285318 | — |
| Product | HCID 22285299 | HCID 22285299 | — |
Reaction Steps
4-(5-Bromo-2-fluorophenyl)pyrimidine (503 mg, 2.0 mmol) was reacted with bis(neopentyl glycolato)diboron (494 mg, 2.2 mmol) using the method in Example 14 part c) to give 4-fluoro-3-pyrimidin-4-yl-phenylboronic acid as a tan solid: m/z (ES+) 219 (M++H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06960598B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-2e057d05e0034238b2de4b86ac785370 |
| Source note | uspto-grants-2005_11 |