HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Iodoanisole → Carbamic acid, (2′-methoxy-3-nitro[1,1′-biphenyl]-4-yl)-, 1,1-dimethylethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Iodoanisole | HCID 68257 | — |
| Reactant | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Product | Carbamic acid, (2′-methoxy-3-nitro[1,1′-biphenyl]-4-yl)-, 1,1-dimethylethyl ester | HCID 69592784 | — |
Reaction Steps
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 2-iodoanisole according to the general procedure C. Obtained as a yellow solid (735 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06960578B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-3296ea50fac845efbe85a778716bba02 |
| Source note | uspto-grants-2005_11 |