HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-iodobenzene → (2'-Chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-iodobenzene | HCID 11993 | — |
| Reactant | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Product | (2'-Chloro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69592813 | — |
Reaction Steps
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1), bis(pinacolato)diboron and 1-chloro-2-iodobenzene according to the general procedure C. Obtained as a yellow oil (886 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06960578B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-35b4bf48515c4c74a13282e6af0f5c1b |
| Source note | uspto-grants-2005_11 |