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HRID1061937

反应详情

EQUATION

反应方程式

HRID 1061937 的结构方程式

REACTANTS

反应物

2
结构：C#C[Si](C)(C)C
HCID66111

Trimethylsilylacetylene

C5H10Si

结构：CC(C)(C)OC(=O)Nc1ccc(I)cc1[N+](=O)[O-]
HCID23554339

Tert-butyl (4-iodo-2-nitrophenyl)carbamate

C11H13IN2O4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1ccc(C#C[Si](C)(C)C)cc1[N+](=O)[O-]
HCID67289195

未命名化合物

收率 107.6%

PROCEDURE

实验过程

Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) (3.64 g, 10 mmol) and trimethylsilylacetylene (4.2 mL, 30 mmol) according to the general procedure F. Obtained as a green oil (3.6 g).