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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1061952Generated: October 31, 2026

Stannous chloride dihydrate → HCID 69592804, compound

https://huagongshe.com/reaction/1061952

Reaction equation

Participants

RoleNameHCIDCharge
ReactantStannous chloride dihydrateHCID 61436—
ReactantHCID 69592859HCID 69592859—
ProductHCID 69592804HCID 6959280474.6%

Reaction Steps

Prepared from (4-(2-chloro-phenylethynyl)-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example F5) (1.61 g, 4.3 mmol) by reduction with SnCl2.2H2O (5.3 g, 23.5 mmol) according to the general procedure G (method b). Obtained as a light brown solid (1.1 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06960578B2
Source datasetuspto-grants-2005_11
ORD IDord-6147818c65aa4ecb8d1243dc45d2b264
Source noteuspto-grants-2005_11