化工社化工社 化学情報印刷レポート · 研究参考用
(2'-Methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester → Carbamic acid,(3-amino-2'-methyl[1,1'-biphenyl]-4-yl)-,1,1-dimethylethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2'-Methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 67290097 | — |
| 触媒 | Nickel | HCID 935 | — |
| 生成物 | Carbamic acid,(3-amino-2'-methyl[1,1'-biphenyl]-4-yl)-,1,1-dimethylethyl ester | HCID 67288955 | — |
反応手順
Prepared from (2′-methyl-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example C9) by catalytic hydrogenation with Raney-Ni according to the general procedure G (method a). Obtained as a white powder (281 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06960578B2 |
| 出典データセット | uspto-grants-2005_11 |
| ORD ID | ord-fe3a1018666f446889ae3b15dba1457f |
| 出典メモ | uspto-grants-2005_11 |