化工社化工社 化学情報印刷レポート · 研究参考用
(2-Nitro-4-pyridin-3-yl-phenyl)-carbamic acid tert.-butyl ester → Tert-butyl 2-amino-4-(pyridin-3-yl)phenylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (2-Nitro-4-pyridin-3-yl-phenyl)-carbamic acid tert.-butyl ester | HCID 69592765 | — |
| 触媒 | Nickel | HCID 935 | — |
| 生成物 | Tert-butyl 2-amino-4-(pyridin-3-yl)phenylcarbamate | HCID 67289423 | — |
反応手順
Prepared from (2-nitro-4-pyridin-3-yl-phenyl)-carbamic acid tert.-butyl ester (Example C10) by catalytic hydrogenation with Raney-Ni according to the general procedure G (method a). Obtained as a grey powder (200 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06960578B2 |
| 出典データセット | uspto-grants-2005_11 |
| ORD ID | ord-63632c0acbc24a9483702079b3be111b |
| 出典メモ | uspto-grants-2005_11 |