HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3'-Fluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester → (3-Amino-3'-fluoro-biphenyl-4-yl)-carbamic acid tert.-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3'-Fluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69592831 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | (3-Amino-3'-fluoro-biphenyl-4-yl)-carbamic acid tert.-butyl ester | HCID 69592797 | — |
Reaction Steps
Prepared from (3′-fluoro-3-nitro-biphenyl-4-yl)-carbamic acid tert.-butyl ester (Example B11) by catalytic hydrogenation with Pd/C according to the general procedure G (method a). Obtained as a brown solid (3.40 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06960578B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-c4746b5b245f403fb3b9ac5ba4340560 |
| Source note | uspto-grants-2005_11 |