HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethyl-6-thiophen-2-yl-[1,3]dioxin-4-one → HCID 86588008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethyl-6-thiophen-2-yl-[1,3]dioxin-4-one | HCID 22224708 | — |
| Reactant | Carbamic acid,(2-amino-4-benzoylphenyl)-,1,1-dimethylethyl ester | HCID 69592848 | — |
| Product | HCID 86588008 | HCID 86588008 | 25.8% |
Reaction Steps
Prepared from (2-amino-4-benzoyl-phenyl)-carbamic acid tert.-butyl ester (Example G24) (259 mg, 0.5 mmol) and 2,2-dimethyl-6-thiophen-2-yl-[1,3]dioxin-4-one (Example J1) (135 mg, 0.55 mmol) according to the general procedure K. Obtained as a light yellow solid (60 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06960578B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-ec090d338a07458d8d63f9dfa9581e49 |
| Source note | uspto-grants-2005_11 |