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HRID1062061

反应详情

EQUATION

反应方程式

HRID 1062061 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)Nc1ccc(C#Cc2ccccc2)cc1N
HCID11404065

1,1-Dimethylethyl N-[2-amino-4-(2-phenylethynyl)phenyl]carbamate

C19H20N2O2

结构：CC1(C)OC(=O)C=C(c2cccc([N+](=O)[O-])c2)O1
HCID22224811

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1ccc(C#Cc2ccccc2)cc1NC(=O)CC(=O)c1cccc([N+](=O)[O-])c1
HCID86588018

未命名化合物

收率 49.5%

PROCEDURE

实验过程

Prepared from (2-amino-4-phenylethynyl-phenyl)-carbamic acid tert.-butyl ester (Example G2) (1.1 g, 4.0 mmol) and 2,2-dimethyl-6-(3-nitro-phenyl)-[1,3]dioxin-4-one (Example J12) (1.23 g, 4.4 mmol) according to the general procedure K. Obtained as a light yellow solid (989 mg).