Water → 2-Bromo-1-(4-methoxyphenyl)-2-(3-pyridyl)ethanone hydrobromide

Beteiligte Stoffe

Reaktionsbedingungen

Reaktionsschritte

1-(4-Methoxyphenyl)-2-(3-pyridyl)ethanone (6.9 g) was dissolved in acetic acid (36 mL), bromine (1.7 mL) was added, and the mixture was stirred at 80° C. for 3 h. The reaction mixture was cooled with iced water and the precipitated crude crystals were collected by filtration. The crude crystals were recrystallized from ethanol-ethyl ether to give the title compound (10 g, yield 89%).

Herkunft & Nachweise