HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl anisate → 2-(4-Chloro-2-pyridinyl)-1-(4-methoxyphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl anisate | HCID 60979 | — |
| Reactant | 4-Chloro-2-methylpyridine | HCID 581392 | — |
| Product | 2-(4-Chloro-2-pyridinyl)-1-(4-methoxyphenyl)ethanone | HCID 21874054 | — |
Reaction Steps
2-(4-Chloro-2-pyridinyl)-1-(4-methoxyphenyl)ethanone was synthesized from 4-chloro-2-picoline (10 g, 78.4 mmol) and ethyl 4-methoxybenzoate (14.1 g, 78.4 mmol) as described in Example 12 to give the product as a mixture of enol and keto tautomers. MS m/z 262 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06962914B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-f4fb6f6ce5154b6b99a4b8d730731d94 |
| Source note | uspto-grants-2005_11 |