HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylfuran-2-carbonyl chloride → HCID 10133382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylfuran-2-carbonyl chloride | HCID 2759851 | — |
| Reactant | 2-Amino-4-methoxy-7-phenyl-benzothiazole | HCID 22283026 | — |
| Product | HCID 10133382 | HCID 10133382 | — |
Reaction Steps
Using 2-amino-4-methoxy-7-phenyl-benzothiazole and freshly prepared 5-methyl-furan-2-carboxylic acid chloride the title compound was obtained crude, which-was chromatographed over SiO2 (Merck 230-400 mesh) eluting with nHexane/EtOAc (4:1), to afford the pure title compound as a pale yellow solid (67% yield), MS: m/e=364.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06963000B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-91095e7a36aa4fc0af9599dab1936fee |
| Source note | uspto-grants-2005_11 |