HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methylthiophene-2-carbonyl chloride → HCID 86584904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methylthiophene-2-carbonyl chloride | HCID 2760083 | — |
| Reactant | HCID 22283057 | HCID 22283057 | — |
| Product | HCID 86584904 | HCID 86584904 | — |
Reaction Steps
Using 4-methoxy-7-phenoxy-benzothiazol-2-ylamine and 5-methyl-thiophene-2-carboxylic acid chloride the title compound was obtained crude, which was chromatographed over SiO2 (Merck 230-400 mesh) eluting with CH2Cl2/EtOAc (1:1), to afford the pure title compound as a pale yellow solid (76% yield), MS: m/e=396.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06963000B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-04f6c0d76da949b29f372a4a96b7cfe3 |
| Source note | uspto-grants-2005_11 |