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HRID1062983

反应详情

EQUATION

反应方程式

HRID 1062983 的结构方程式

REACTANTS

反应物

2
结构：Cc1c[c]([Sn]([CH3])([CH3])[CH3])ccn1
HCID12691320

2-Methyl-4-(trimethylstannyl)pyridine

C9H15NSn

结构：COc1ccc(I)c2sc(NC(=O)c3ccc(C)s3)nc12
HCID86584906

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(-c2ccnc(C)c2)c2sc(NC(=O)c3ccc(C)s3)nc12
HCID10111310

未命名化合物

收率 50%

PROCEDURE

实验过程

5-Methyl-thiophene-2-carboxylic acid [4-methoxy-7-(2-methyl-pyridin-4-yl)-benzothiazol-2-yl]-amide is synthesized from 5-methyl-thiophene-2-carboxylic acid (4-methoxy-7-iodo-benzothiazol-2-yl)-amide (260 mg, 0.60 mmol) and 2-methyl-4-trimethylstannanyl-pyridine (384 mg, 0.90 mmol) using the general procedure B as a light yellow solid in 50% yield. MS: m/e=396 (M+H+).