Ethylamine → HCID 69736414, compound

HRID 1063134Notes

Reaction equation

HRID 1063134 reaction equation
[CH2:1]([NH2:3])[CH3:2].[Cl:4][C:5]1[CH:10]=[CH:9][N:8]=[C:7]2[CH:11]=[C:12]([C:14]([O-])=[O:15])[S:13][C:6]=12.[Li+]>>[CH2:1]([NH:3][C:14]([C:12]1[S:13][C:6]2[C:7](=[N:8][CH:9]=[CH:10][C:5]=2[Cl:4])[CH:11]=1)=[O:15])[CH3:2]

Participants

3

Reactant 2

HCID 6341EthylamineHCID 23677819Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate

Product 1

HCID 69736414HCID 69736414, compound

Procedure

The title compound was prepared from ethylamine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: n.d.; HPLC Rf: 4.18 min; HPLC purity: 98%.

Sources & evidence

ORD record
ord-b1b5db4fb85448b29cb4d254df291dd8
Source dataset
uspto-grants-2005_11
Patent number
US06964961B2

Reaction notes

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