1-(3-Aminopropyl)-4-methylpiperazine → HCID 91335553, compound

HRID 1063148Notes

Reaction equation

HRID 1063148 reaction equation
[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([CH2:8][CH2:9][CH2:10][NH2:11])[CH2:4][CH2:3]1.[Cl:12][C:13]1[CH:18]=[CH:17][N:16]=[C:15]2[CH:19]=[C:20]([C:22]([O-])=[O:23])[S:21][C:14]=12.[Li+]>>[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([CH2:8][CH2:9][CH2:10][NH:11][C:22]([C:20]2[S:21][C:14]3[C:15](=[N:16][CH:17]=[CH:18][C:13]=3[Cl:12])[CH:19]=2)=[O:23])[CH2:4][CH2:3]1

Participants

3

Reactant 2

HCID 783281-(3-Aminopropyl)-4-methylpiperazineHCID 23677819Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate

Product 1

HCID 91335553HCID 91335553, compound

Procedure

The title compound was prepared from 3-(4-methylpiperazin-1-yl)-propylamine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: 353/355 (MH+); HPLC Rf: n.d.; HPLC purity: n.d.

Sources & evidence

ORD record
ord-7af260d248f146dba188c008208ee7f5
Source dataset
uspto-grants-2005_11
Patent number
US06964961B2

Reaction notes

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