HCID 22278663, compound → HCID 85797601, compound

HRID 1063154Notes

Reaction equation

HRID 1063154 reaction equation
N1C=CC=CC=1.[N:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:13][CH2:14][NH2:15].[Cl:16][C:17]1[CH:22]=[CH:21][N:20]=[C:19]2[CH:23]=[C:24]([C:26]([O-])=[O:27])[S:25][C:18]=12.[Li+]>>[N:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[CH2:13][CH2:14][NH:15][C:26]([C:24]1[S:25][C:18]2[C:19](=[N:20][CH:21]=[CH:22][C:17]=2[Cl:16])[CH:23]=1)=[O:27]

Participants

3

Reactant 2

HCID 22278663HCID 22278663, compoundHCID 23677819Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate

Product 1

HCID 85797601HCID 85797601, compound

Procedure

The title compound was prepared from 2-pyridine-2-yl-ethylamine pyridine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: 318/320 (MH+); HPLC Rf: 4.33 min.; HPLC purity: 97%.

Sources & evidence

ORD record
ord-9181a038f8504324a60d3ac418d9ffc6
Source dataset
uspto-grants-2005_11
Patent number
US06964961B2

Reaction notes

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