4-Pyridineethanamine → HCID 85797606, compound

HRID 1063160Notes

Reaction equation

HRID 1063160 reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][NH2:9])=[CH:3][CH:2]=1.[Cl:10][C:11]1[CH:16]=[CH:15][N:14]=[C:13]2[CH:17]=[C:18]([C:20]([O-])=[O:21])[S:19][C:12]=12.[Li+]>>[N:1]1[CH:6]=[CH:5][C:4]([CH2:7][CH2:8][NH:9][C:20]([C:18]2[S:19][C:12]3[C:13](=[N:14][CH:15]=[CH:16][C:11]=3[Cl:10])[CH:17]=2)=[O:21])=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 832754-PyridineethanamineHCID 23677819Lithium 7-chlorothieno[3,2-b]pyridine-2-carboxylate

Product 1

HCID 85797606HCID 85797606, compound

Procedure

The title compound was prepared from 2-pyridin-4-yl-ethyl amine and lithium 7-chloro-thieno[3,2-b]pyridine-2-carboxylate by a procedure analogous to Example 1B. MS: 318/320 (MH+); HPLC Rf: 4.08 min.; HPLC purity 99%.

Sources & evidence

ORD record
ord-44d1de05628647abaf77334e2a261662
Source dataset
uspto-grants-2005_11
Patent number
US06964961B2

Reaction notes

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