HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-1-benzyl-3-ethyl-3-methylpiperidine → HCID 22278891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-1-benzyl-3-ethyl-3-methylpiperidine | HCID 22278895 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 22278891 | HCID 22278891 | — |
Reaction Steps
A mixture of 20% Pd(OH)2 on carbon (0.2 g) and 4-amino-1-benzyl-3-ethyl-3-methylpiperidine (0.6 g, 2.58 mmol) in methanol (210 ml) was stirred in hydrogen atmosphere (1 atm.) at 30° C. for 6 hr. The catalyst was filtered off, washed with methanol and filtrate was concentrated to dryness to afford 4-amino-3-ethyl-3-methylpiperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06964966B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-3dcd541b0ac9426aaafcac3d38b482f7 |
| Source note | uspto-grants-2005_11 |