HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 9965731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | 4-Nitrobenzyl bromide | HCID 66011 | — |
| Product | HCID 9965731 | HCID 9965731 | 79% |
Reaction Steps
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (2.00 g, 13.0 mmole) and 4-nitrobenzyl bromide (3.38 g, 15.6 mmole), 2.90 g (79% yield) of 5-(4-nitrobenzyl)aminosalicylic acid was obtained as a pale yellow solid.: mp 211-212° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06964982B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-a826bd1c130b41579aa471ad7ceb1113 |
| Source note | uspto-grants-2005_11 |