Nitric Acid → HCID 69732814, compound

Participants

Reaction Steps

Into a flask were charged 100 g of 9-ethylcarbazole and 245 g of o-dichlorobenzene, and then nitration was carried out using nitric acid. The reaction solution was neutralized, and the oil layer separated was washed with water to provide 370 g of an o-dichlorobenzene solution of nitroethylcarbazole. The yield of 3-nitro-9-ethylcarbazoic was 90%. The resulting solution contained 110 g of 3-nitro-9-ethylcarbazole, 8 g of 1-nitro-9-ethylcarbazole. The content of the nitrate was 250 ppm.

Provenance & Evidence