HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Diethylphosphonomethyloxy-5-methoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | 2-Diethylphosphonomethyloxy-5-methoxynitrobenzene | HCID 54481034 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Diethylphosphonomethyloxy-5-methoxyaniline | HCID 54383135 | — |
Reaction Steps
A solution of SnCl2 (4 mmole) in freshly prepared methonolic HCl (10 mL) was added to a cold (0° C.) solution of 2-diethylphosphonomethyloxy-5-methoxynitrobenzene (1 mmole) in MeOH (5 mL). The mixture was warmed to room temperature and stirred for 3 h. Evaporation, extraction and chromatography provided 2-diethylphosphonomethyloxy-5-methoxyaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06965033B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-4a12314f686a418da760f4c2717930b2 |
| Source note | uspto-grants-2005_11 |