4-(bromomethyl)-3-(2,6-dichlorophenyl)-5-methylisoxazole → HCID 22280010, compound
Reaction equation
Br[CH2:2][C:3]1[C:4]([C:9]2[C:14]([Cl:15])=[CH:13][CH:12]=[CH:11][C:10]=2[Cl:16])=[N:5][O:6][C:7]=1[CH3:8].C[O:18][C:19](=[O:32])[CH2:20][O:21][C:22]1[CH:30]=[CH:29][C:28]([SH:31])=[C:27]2[C:23]=1[CH2:24][CH2:25][CH2:26]2>>[Cl:16][C:10]1[CH:11]=[CH:12][CH:13]=[C:14]([Cl:15])[C:9]=1[C:4]1[C:3]([CH2:2][S:31][C:28]2[CH:29]=[CH:30][C:22]([O:21][CH2:20][C:19]([OH:32])=[O:18])=[C:23]3[C:27]=2[CH2:26][CH2:25][CH2:24]3)=[C:7]([CH3:8])[O:6][N:5]=1Participants
3
Procedure
The title compound was prepared in the manner analogous to Example 1F using commercially available 4-bromomethyl-3-(2,6-dichloro-phenyl)-5-methyl-isoxazole and 12C. MS m/z 478 (M+1).
Sources & evidence
- ORD record
- ord-3d44f8013d6f497aae1d0669879ebfcd
- Source dataset
- uspto-grants-2005_11
- Patent number
- US06964983B2
Reaction notes
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