HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide → HCID 22275899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 23401683 | HCID 23401683 | — |
| Product | HCID 22275899 | HCID 22275899 | 86% |
Reaction Steps
4-chloro-N-(2,5-dichlorophenyl)-N-[4-[[(1,1-dimethylethyl)carbonyl]amino]-1-methylbutyl]benzenesulfonamide was prepared analogous to 4-chloro-N-[2,5-dichlorophenyl]-N-[(R)-1-methyl-4-(acetylamino)butyl]benzenesulfonamide by reacting 4-chloro-N-[2,5-dichlorophenyl]-N-[R]-1-methyl-4-aminobutyl]benzenesulfonamide with pivaloyl chloride. Yield=86%; MS (ESI+), 505 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-ada311ee00674b26a48373a2ca8adcea |
| Source note | uspto-grants-2005_11 |