HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide → HCID 23401693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | HCID 23401683 | HCID 23401683 | — |
| Product | HCID 23401693 | HCID 23401693 | 82% |
Reaction Steps
4-chloro-N-(2,5-dichlorophenyl)-N-[4-[[(phenoxy)carbonyl]amino]-1(R)-methylbutyl]benzenesulfonamide was prepared analogous to 4-chloro-N-[2,5-dichlorophenyl]-N-[(R)-1-methyl (acetylamino)butyl]benzenesulfonamide by reacting 4-chloro-N-[2,5-dichlorophenyl]-N-[R]-]-methyl-4-aminobutyl]benzenesulfonamide with phenyl chloroformate. Yield=82%; MS (ESI+), 541 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-07d2f90b90f24205827e9ddf702c4b50 |
| Source note | uspto-grants-2005_11 |