HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 23401687, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 1-Pentanesulfonyl chloride | HCID 237555 | — |
| Reactant | HCID 53796417 | HCID 53796417 | — |
| Product | HCID 23401687 | HCID 23401687 | 59% |
Reaction Steps
4-chloro-N-[2,5-dichlorophenyl]-N-[4-(diethylaminosulfonyl)-1(R)-methylbutyl]-benzenesulfonamide was prepared analogous to 4-chloro-N-[2,5-dichlorophenyl]-N-[4-[(methylamino)sulfonyl]-1(R)-methylbutyl]benzenesulfonamide by reacting (4R)-4-[2,5-dichlorophenyl][4-chlorophenyl)sulfonyl]-amino]pentylsulfonyl chloride with diethylamine. Yield=59%; MS (ESI+), 541 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-19aa3bb08d4549018574ffb412ae3b27 |
| Source note | uspto-grants-2005_11 |