HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine → HCID 23401680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine | HCID 67164 | — |
| Reactant | 1-Pentanesulfonyl chloride | HCID 237555 | — |
| Reactant | HCID 53796417 | HCID 53796417 | — |
| Product | HCID 23401680 | HCID 23401680 | 64% |
Reaction Steps
4-chloro-N-[2,5-dichlorophenyl]-N-[4[(4-thiomorpholinyl)sulfonyl]-1(R)-methylbutyl]benzenesulfonamide was prepared analogous to 4-chloro-N-[2,5-dichlorophenyl]-N-[4-[(methylamino)sulfonyl]-1(R)-methylbutyl]benzenesulfonamide by reacting (4R)-4-[2,5-dichlorophenyl][4-chlorophenyl)sulfonyl]-amino]pentylsulfonyl chloride with thiomorpholine. Yield=64%; MS (ESI+), 571 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967196B1 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-acdd74315c1e479ab569629d8882a388 |
| Source note | uspto-grants-2005_11 |