HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 2-Acetamidodibenzothiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Dibenzothiophenamine | HCID 298442 | — |
| Product | 2-Acetamidodibenzothiophene | HCID 108627 | — |
Reaction Steps
The title compound was prepared following the procedure of Example 2 using 2-aminodibenzthiophene (Bull. Soc. Chim. Fr. (1996), 133(6), 597-610) and acetyl chloride. NMR: 10.13 (brs, 1H), 8.6 (d, 1H), 8.15 (m, 1H), 8.0 (m, 1H), 7.9 (d, 1H), 7.6 (dd, 1H), 7.5 (m, 2H), 2.1 (s, 3H); m/z 242.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06967216B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-97d46ed1c2b1486398122dc0192ba12d |
| Source note | uspto-grants-2005_11 |