Zirconium → HCID 131725226, compound

HRID 1064213Notes

Reaction equation

HRID 1064213 reaction equation
[CH3:1][N+:2]([CH2:5][C:6]([O-:8])=[O:7])([CH3:4])[CH3:3].O.[Zr:10].O(Cl)Cl.[Zr].ClO.[Al:17]>>[Zr:10].[Al:17].[CH3:1][N+:2]([CH2:5][C:6]([OH:8])=[O:7])([CH3:4])[CH3:3]

Participants

5

Reactant 4

HCID 23995ZirconiumHCID 24884197Betaine monohydrateHCID 569243881327-41-92×HCID 71304769Chloro hypochlorite;zirconium

Product 1

HCID 131725226HCID 131725226, compound

Procedure

Betaine monohydrate powder (287 g) is added to a zirconium compound (1000 g of a 31% solution of zirconium oxychloride (ZrOCl2)) with stirring. Aluminum chlorohydrate (“ACH”) (2800 g of a 20% ACH solution made from a powder (REACH 101, from Reheis, Berkeley Height, N.J.) is then added with additional stirring. The final solution is then quickly spray dried to remove water. The Zirconium/Aluminum/Betaine (“ZAB”) powder obtained has a Betaine/zirconium molar ratio of 1.42:1; an aluminum:zirconium molar ratio of 3.56:1; and a metal:chloride ratio of 1.05:1.

Workup

  1. additionis then added with additional stirring
  2. dry with materialThe final solution is then quickly spray dried
  3. customto remove water

Sources & evidence

ORD record
ord-72e5d036e4a94cf38c7f6d45ed139990
Source dataset
uspto-grants-2005_11
Patent number
US06969510B2

Reaction notes

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