Propan-2-yl 2,3,3,3-tetrafluoro-2-(heptafluoropropoxy)propanoate → (CF3)2Cfococf(CF3)ocf2CF2CF3

Participants

Reaction Steps

Further, the same operation was repeated once. The total amount of benzene injected was 0.219 g, and the total amount of R-113 injected was 21 ml. Further, nitrogen was supplied for 1.5 hours. The product was quantified by 19F-NMR, whereby the yield of the above identified compound to (CH3)2CHOCOCF(CF3)OCF2CF2CF3, was 48.1%, and the yield of (CF3)2CHOCOCF(CF3)OCF2CF2CF3 to (CH3)2CHOCOCF(CF3)OCF2CF2CF3, was 19.1%.

Provenance & Evidence