2-Chloro-N-(2,6-dimethylphenyl)acetamide → HCID 10132663, compound

HRID 1064562Notes

Reaction equation

HRID 1064562 reaction equation
[CH3:1][CH:2]1[N:7]([C:8]2[CH:13]=[CH:12][C:11]([CH3:14])=[CH:10][CH:9]=2)[CH2:6][CH2:5][NH:4][CH2:3]1.Cl[CH2:16][C:17]([NH:19][C:20]1[C:25]([CH3:26])=[CH:24][CH:23]=[CH:22][C:21]=1[CH3:27])=[O:18]>>[CH3:1][CH:2]1[N:7]([C:8]2[CH:13]=[CH:12][C:11]([CH3:14])=[CH:10][CH:9]=2)[CH2:6][CH2:5][N:4]([CH2:16][C:17]([NH:19][C:20]2[C:25]([CH3:26])=[CH:24][CH:23]=[CH:22][C:21]=2[CH3:27])=[O:18])[CH2:3]1

Participants

3

Reactant 2

HCID 707982-Chloro-N-(2,6-dimethylphenyl)acetamideHCID 982902-Methyl-1-(4-methylphenyl)piperazine

Product 1

HCID 10132663HCID 10132663, compound

Procedure

The title compound was prepared from (±)-3-methyl-4-(4-methylphenyl)piperazine (0.1 g) and 2-chloro-N-(2,6-dimethylphenyl)acetamide (0.1 g) by the method of Example 1 step (iii) as a white solid. Yield 0.056 g.

Sources & evidence

ORD record
ord-c5605638fd47430da5ba531d143f5a4b
Source dataset
uspto-grants-2005_11
Patent number
US06969713B2

Reaction notes

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