4-Cyanobenzenesulfonyl chloride → HCID 69745203, compound

HRID 1064586Notes

Reaction equation

HRID 1064586 reaction equation
[CH3:1][C@H:2]1[NH:7][C@@H:6]([CH3:8])[CH2:5][N:4]([CH2:9][C:10]([NH:12][C:13]2[CH:22]=[CH:21][CH:20]=[C:19]3[C:14]=2[CH:15]=[CH:16][CH:17]=[N:18]3)=[O:11])[CH2:3]1.[C:23]([C:25]1[CH:30]=[CH:29][C:28]([S:31](Cl)(=[O:33])=[O:32])=[CH:27][CH:26]=1)#[N:24]>>[CH3:1][C@H:2]1[N:7]([S:31]([C:28]2[CH:27]=[CH:26][C:25]([C:23]#[N:24])=[CH:30][CH:29]=2)(=[O:33])=[O:32])[C@@H:6]([CH3:8])[CH2:5][N:4]([CH2:9][C:10]([NH:12][C:13]2[CH:22]=[CH:21][CH:20]=[C:19]3[C:14]=2[CH:15]=[CH:16][CH:17]=[N:18]3)=[O:11])[CH2:3]1

Participants

3

Reactant 2

HCID 394974-Cyanobenzenesulfonyl chlorideHCID 69745804HCID 69745804, compound

Product 1

HCID 69745203HCID 69745203, compound

Procedure

The title compound was prepared from the product of Example 58 step (i) (0.503 mmol) and 4-cyanobenzenesulphonyl chloride (0.503 mmol) by the method of Example 58 step (ii) as a white solid. Yield: 4 mg

Sources & evidence

ORD record
ord-0077c2a334d749d4bdceb3f29b99c3d0
Source dataset
uspto-grants-2005_11
Patent number
US06969713B2

Reaction notes

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