2-Methanesulfonylbenzene-1-sulfonyl chloride → HCID 60045701, compound

HRID 1064592Notes

Reaction equation

HRID 1064592 reaction equation
[CH3:1][C@H:2]1[NH:7][C@@H:6]([CH3:8])[CH2:5][N:4]([CH2:9][C:10]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[C:14]=2[CH3:21])=[O:11])[CH2:3]1.[CH3:22][S:23]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[S:32](Cl)(=[O:34])=[O:33])(=[O:25])=[O:24]>>[CH3:22][S:23]([C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[S:32]([N:7]1[C@@H:6]([CH3:8])[CH2:5][N:4]([CH2:9][C:10]([NH:12][C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[C:14]=2[CH3:21])=[O:11])[CH2:3][C@H:2]1[CH3:1])(=[O:34])=[O:33])(=[O:25])=[O:24]

Participants

3

Reactant 2

HCID 27351782-Methanesulfonylbenzene-1-sulfonyl chlorideHCID 69745130HCID 69745130, compound

Product 1

HCID 60045701HCID 60045701, compound

Procedure

The title compound was prepared from the product of step (i) (0.503 mmol) and 2-methanesulphonylbenzenesulphonyl chloride (0.503 mmol) by the method of Example 58 step (ii) as a white solid. Yield: 6 mg

Sources & evidence

ORD record
ord-cc08248eef7a4929a8b2358e5a81c23e
Source dataset
uspto-grants-2005_11
Patent number
US06969713B2

Reaction notes

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