4-Cyanobenzenesulfonyl chloride → HCID 69745153, compound

HRID 1064602Notes

Reaction equation

HRID 1064602 reaction equation
[CH3:1][C@H:2]1[NH:7][CH2:6][CH2:5][N:4]([CH2:8][C:9]([NH:11][C:12]2[CH:21]=[CH:20][CH:19]=[C:18]3[C:13]=2[CH:14]=[CH:15][CH:16]=[N:17]3)=[O:10])[CH2:3]1.[C:22]([C:24]1[CH:29]=[CH:28][C:27]([S:30](Cl)(=[O:32])=[O:31])=[CH:26][CH:25]=1)#[N:23]>>[C:22]([C:24]1[CH:25]=[CH:26][C:27]([S:30]([N:7]2[CH2:6][CH2:5][N:4]([CH2:8][C:9]([NH:11][C:12]3[CH:21]=[CH:20][CH:19]=[C:18]4[C:13]=3[CH:14]=[CH:15][CH:16]=[N:17]4)=[O:10])[CH2:3][C@H:2]2[CH3:1])(=[O:32])=[O:31])=[CH:28][CH:29]=1)#[N:23]

Participants

3

Reactant 2

HCID 394974-Cyanobenzenesulfonyl chlorideHCID 69746584HCID 69746584, compound

Product 1

HCID 69745153HCID 69745153, compound

Procedure

The title compound was prepared from the product of step (i) (1.4 g) and 4-cyanobenzenesulphonyl chloride (1 g) by the method of Example 58 step (ii) as a white solid. Yield: 0.41 g

Sources & evidence

ORD record
ord-173b8d014ecc449092e1cb5fcc726353
Source dataset
uspto-grants-2005_11
Patent number
US06969713B2

Reaction notes

Loading…