Chloroacetyl chloride → HCID 22273464, compound

HRID 1064605Notes

Reaction equation

[CH3:1][S:2]([C:5]1[CH:6]=[CH:7][C:8]([CH3:12])=[C:9]([CH:11]=1)[NH2:10])(=[O:4])=[O:3].[Cl:13][CH2:14][C:15](Cl)=[O:16]>>[Cl:13][CH2:14][C:15]([NH:10][C:9]1[CH:11]=[C:5]([S:2]([CH3:1])(=[O:3])=[O:4])[CH:6]=[CH:7][C:8]=1[CH3:12])=[O:16]

Participants

Reactant 2

HCID 6577Chloroacetyl chloride

HCID 175119545-Methanesulfonyl-2-methylaniline

Product 1

HCID 22273464HCID 22273464, compound

Procedure

The subtitle compound was prepared from 5-methanesulphonyl-2-methylaniline (0.82 g) and chloroacetyl chloride (0.72 ml) by the method of Example 33 step (iii) as a beige solid. Yield: 0.61 g

Sources & evidence

ORD record: ord-c09b780dea454ee7ad4fe73f473928ab
Source dataset: uspto-grants-2005_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06969713B2

Reaction notes

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