HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3S)-(-)-3-(Dimethylamino)pyrrolidine → HCID 10067030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3S)-(-)-3-(Dimethylamino)pyrrolidine | HCID 7019156 | — |
| Reactant | 2-[5-(4-cyanophenyl)-1-benzofuran-2-yl]ethyl Methanesulfonate | HCID 11393678 | — |
| Product | HCID 10067030 | HCID 10067030 | — |
Reaction Steps
The product from Example 1C and 3-(S)-(dimethylamino)pyrrolidine were processed as described in Example 1D to provide the titled compound. 1H NMR (300 MHz, CD3OD) 67 7.88 (m, 1H), 7.80 (m, 4H), 7.58 (m, 2H), 6.80 (s, 1H), 4.43 (m, 1H), 3.6-3.9 (m, 4H), 3.35-3.45 (m, 4H), 2.95 (s, 6H), 2.6 (m, 1H), 2.35 (m, 1H); MS (DCI) m/z 360 (M+H)+;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06969730B2 |
| Source dataset | uspto-grants-2005_11 |
| ORD ID | ord-4799ba0a3e4244b7a8dbaea26b152176 |
| Source note | uspto-grants-2005_11 |