HCID 11234748, compound → HCID 10133949, compound

Participants

Reaction Steps

The product from Example 145 and cyclopropylmagnesium bromide were processed as described in Example 146 to provide the title compound (48% yield). MS (ESI APCI) m/z 374 (M+H)+; 1HNMR (300 MHz, CD3OD) δ 1.08-1.22 (m, 7 H), 1.39-1.53 (m, 1 H), 1.73-1.86 (m, 2 H), 1.95-2.08 (m, 1 H), 2.23-2.35 (m, 1 H), 2.41-2.60 (m, 2 H), 2.87-3.15 (m, 3H), 3.19-3.35 (m, 2 H), 6.63 (s, 1 H), 7.48-7.55 (m, 2 H), 7.60,(dd, 1 H), 7.78-7.81 (m, 1 H), 7.89 (ddd, 1 H), 8.02 (ddd, 1 H), 8.25 (dd, 1 H).

Provenance & Evidence