Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trimethoxysilane | HCID 17215 | — |
| Reactant | Phenol, 3-(2-propen-1-yloxy)-, 1-benzoate | HCID 11448176 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20509689 | HCID 20509689 | — |
Reaction Steps
A mixture of 25.4 g. (0.1 mole) of 3-allyloxyphenyl benzoate, 50 ml. of dry toluene, 20 g. (0.15 mole) of trimethoxysilane and 2 drops of platinum hydrosilation catalyst is heated at 90° C. for 17 hours under nitrogen. After the reaction mixture is cooled to about 20° C., it is concentrated under reduced pressure to produce the uv precursor product. For purification, the product is passed through a short silica column using dichloromethane as an eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04328346 |
|---|
| Source dataset | uspto-grants-1982_05 |
|---|
| ORD ID | ord-6369434f748747dca8c8b3a7b290b164 |
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| Source note | uspto-grants-1982_05 |
|---|
