Water → 1,1'-{4-(Ethylamino)-6-[(prop-2-en-1-yl)oxy]-1,3-phenylene}di(ethan-1-one)

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Reaction Steps

Allyl bromide (2 g) was added to a stirred solution of 4,6-diacetyl-3-ethylaminophenol (0.016 M) in dimethylformamide (30 ml) containing potassium carbonate (2 g). The mixture was heated at 60°-70° C. for two hours, and was then poured into water (100 ml), stirred, and the precipitated product isolated by filtration. Yield 93%, mp 82°-83° C.

Provenance & Evidence