HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 20541594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | (3-Bromopropyl)benzene | HCID 12503 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20541594 | HCID 20541594 | — |
Reaction Steps
17 parts by weight of cyclohexene are added dropwise at +10° C. to a mixture of 40 parts by weight of 3-phenylpropyl bromide and 20 parts by weight of 96% strength sulfuric acid. Stirring is continued for 14 hours at room temperature. The crude product is dissolved in CHCl3 and the solution is thoroughly washed with ice water, dried over Na2CO3 and distilled. 35 parts by weight of 3-(4-cyclohexylphenyl)-propyl bromide are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04328380 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-06d073b230584775a5cb4c560da0ba97 |
| Source note | uspto-grants-1982_05 |