HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 20541604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | (3-Chloropropyl)benzene | HCID 7706 | — |
| Reactant | Cyclohexene | HCID 8079 | — |
| Product | HCID 20541604 | HCID 20541604 | 57% |
Reaction Steps
16.5 parts by weight of cyclohexene are added dropwise at +10° C. to a mixture of 31 parts by weight of 3-phenylpropyl chloride and 20 parts by weight of 96% strength sulfuric acid. Stirring is continued for 14 hours at room temperature. The crude product is dissolved in CHCl3 /ice water and the organic solution is thoroughly washed with ice water, dried over Na2CO3 and distilled. 27 parts by weight of 3-(4-cyclohexylphenyl)-propyl chloride are obtained; boiling point 126° C.-130° C./0.2 mm Hg, yield 57%(based on 3-phenylpropyl chloride).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04328380 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-c52ea3062d774773b4859aa1555faa2a |
| Source note | uspto-grants-1982_05 |